Skip to main content
Prosiding Dataverse (LIPI)
The Synthesis of Calcium Salt from Brine Water by Partial Evaporation and Chemical Precipitation
Version 2.0
The Synthesis of Calcium Salt from Brine Water by Partial Evaporation and Chemical Precipitation
Lalasari, L. H.; Widowati, M. K.; Natasha, N. C.; Sulistiyono, E.; Prasetyo, A. B., 2018, "The Synthesis of Calcium Salt from Brine Water by Partial Evaporation and Chemical Precipitation", https://hdl.handle.net/20.500.12690/RIN/IHGIEB, RIN Dataverse, V2
Learn about Data Citation Standards.
Contact Owner Share
Dataset Metrics
0 Views
0 Downloads
Description

In this study would be investigated the effects of partial evaporation and chemical precipitation in the formation of calcium salt from brine water resources. The chemical reagents used in the study was oxalate acid (C2H2O4), ammonium carbonate (NH4)2CO3) and ammonium hydroxide (NH4OH) with reagent concentration of 2 N, respectively. The procedure was 10 liters brine water evaporated until 20 persen volume and continued with filtration process to separate brine water filtrate from residue (salt). Salt resulted from evaporation process was characterized by Scanning Electron Microscopy (SEM), X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD) techniques. Filtrate then was reacted with C2H2O4, (NH4)2CO3 and NH4OH reagents to get salt products in atmospheric condition and variation ratio volume brine water/chemicals (v/v) [10/1; 10/5; 10/10; 10/20; 10/30; 10:50; 20/1; 20/5; 20/10; 20/20; 20/30; 20:50]. The salt product than were filtered, dried, measured weights and finally characterized by SEM/EDS and XRD techniques. The result of experiment showed the chemical composition of brine water from Tirta Sanita, Bogor was 28.87 persen Na, 9.17 persen Mg, 2.94 persen Ca, 22.33 persen O, 0.71 persen Sr, 30.02 persen Cl, 1.51 persen Si, 1.23 persen K, 0.55 persen S, 1.31 persen Al. The chemical composition of salt resulted by partial evaporation was 53.02 persen Ca, 28.93 persenO, 9.50 persen Na, 2.10 persen Mg, 1.53 persen Sr, 1.20 persen Cl, 1.10 persen Si, 0.63 persen K, 0.40 persen S, 0.39 persen Al. The salt resulted by total evaporation was indicated namely as NaCl. Whereas salt resulted by partial evaporation was CaCO3 with a purity of 90 persen from High Score Plus analysis. In the experiment by chemical precipitation was reported that the reagents of ammonium carbonate were more reactive for synthesizing calcium salt from brine water compared to reagents of oxalate acid and ammonium hydroxide. The salts precipitated by NH4OH, (NH4)2CO3, and H2C2O4 reagents were indicated as NaCl, CaCO3 and CaC2O4.H2O, respectively. The techniques of partial evaporation until 20 persen volume sample of brine water and chemical precipitation using (NH4)2CO3 reagent are recommended in the synthesis of calcium salts from brine water because are simple, flexible and economical.

IOP Conf. Series: Materials Science and Engineering 17 6 (2017 ) 012040

(2017)
Subject Physics
Filter by
1 to 10 of 10 Files
The Synthesis of Calcium Salt from Brine Water by Partial Evaporation and Chemical Precipitation.pdf
The Synthesis of Calcium Salt from Brine Water by Partial Evaporation and Chemical Precipitation.pdf
Adobe PDF - 793.6 KB
Published May 24, 2018
2 Downloads
MD5: d6f8d5a7c920f8c026438063bd658b5c
Figure 1.Brine water sample.JPG
Figure 1.Brine water sample.JPG
JPEG Image - 24.7 KB
Published Nov 15, 2018
1 Download
MD5: cc971080cd8f82eb5f851e2e21ab42b8
Figure 1.Brine water sample
Data
Figure 3. The flowchart of research.JPG
Figure 3. The flowchart of research.JPG
JPEG Image - 45.4 KB
Published Nov 15, 2018
1 Download
MD5: fd760011f49e3dad3469a092a8244700
Figure 3. The flowchart of research
Data
Figure 4. The morphology of residue product on evaporation.JPG
Figure 4. The morphology of residue product on evaporation.JPG
JPEG Image - 37.1 KB
Published Nov 15, 2018
1 Download
MD5: 4c132c6120179b4ad75eddae4896eb29
Figure 4. The morphology of residue product on evaporation: (a) total evaporation; (b) partial evaporation (evaporation until 20% volume sample)
Data
Figure 6. The morphology of brine salt by chemical precipitation using.JPG
Figure 6. The morphology of brine salt by chemical precipitation using.JPG
JPEG Image - 43.6 KB
Published Nov 15, 2018
1 Download
MD5: 3158e53fff6143617189f8b96c25bacf
Figure 6. The morphology of brine salt by chemical precipitation using: (a) Oxalate acid; (b) Ammonium carbonate; (c) Ammonium hydroxide
Data
Table 1. The chemical composition of brine water.JPG
Table 1. The chemical composition of brine water.JPG
JPEG Image - 22.0 KB
Published Nov 15, 2018
1 Download
MD5: 469aab6ffc581bbed68dd0faf6ea9568
Table 1. The chemical composition of brine water
Data
Table 2. The chemical composition of brine water and residue by.JPG
Table 2. The chemical composition of brine water and residue by.JPG
JPEG Image - 34.6 KB
Published Nov 15, 2018
1 Download
MD5: 747976fc134ebee2c0da8e8a5a68b559
Table 2. The chemical composition of brine water and residue by partial evaporation until 20% (v/v) sample
Data
Table 3. The solubility product (Ksp) of brine salt product.JPG
Table 3. The solubility product (Ksp) of brine salt product.JPG
JPEG Image - 50.3 KB
Published Nov 15, 2018
1 Download
MD5: d47ee498c5d3869344d5614cff8387c7
Table 3. The solubility product (Ksp) of brine salt product
Data
Table 4. The formation of salt from the concentrated brine water in variation ratio volume (vv).JPG
Table 4. The formation of salt from the concentrated brine water in variation ratio volume (vv).JPG
JPEG Image - 66.9 KB
Published Nov 15, 2018
1 Download
MD5: 2a6d948aa9886ae2af35bd76d7d1d0e9
Table 4. The formation of salt from the concentrated brine water in variation ratio volume (v/v) concentrated brine water (filtrate)/reagents and variation reagents
Data
Table 5. The semi quantitative of chemical composition from salt brine by EDS-SEM.JPG
Table 5. The semi quantitative of chemical composition from salt brine by EDS-SEM.JPG
JPEG Image - 41.7 KB
Published Nov 15, 2018
1 Download
MD5: f624e6fe8ff1dfaa24a15931554fec1d
Table 5. The semi quantitative of chemical composition from salt brine by EDS-SEM
Data
Edit File

This file has already been deleted (or replaced) in the current version. It may not be edited.

Restrict Files and Add Dataset Terms of Access

Restricting limits access to published files. You can add or edit Terms of Access for the dataset, and allow people to Request Access to restricted files.

Enable access request
Delete Files

The file will be deleted after you click on the Delete button.

Files will not be removed from previously published versions of the dataset.

Select File(s)

Please select one or more files.

Share Dataset

Share this dataset on your favorite social media networks.

Dataset Citations

Citations for this dataset are retrieved from Crossref via DataCite using Make Data Count standards. For more information about dataset metrics, please refer to the User Guide.

Sorry, no citations were found.
Restricted Files Selected

The restricted file(s) selected may not be downloaded because you have not been granted access.

Restricted Files Selected

The restricted file(s) selected may not be downloaded because you have not been granted access.

Click Continue to download the files you have access to download.

Restricted Files Selected

The restricted file(s) selected may not be downloaded because you have not been granted access.

Click Continue to download the files you have access to download.

Delete Dataset

Are you sure you want to delete this dataset and all of its files? You cannot undelete this dataset.

Delete Draft Version

Are you sure you want to delete this draft version? Files will be reverted to the most recently published version. You cannot undelete this draft.

Unpublished Dataset Private URL

Private URL can only be used with unpublished versions of datasets.

Unpublished Dataset Private URL

Are you sure you want to disable the Private URL? If you have shared the Private URL with others they will no longer be able to use it to access your unpublished dataset.

Delete Files

The file(s) will be deleted after you click on the Delete button.

Files will not be removed from previously published versions of the dataset.

Compute

This dataset contains restricted files you may not compute on because you have not been granted access.

Deaccession Dataset

Are you sure you want to deaccession? The selected version(s) will no longer be viewable by the public.

Deaccession Dataset

Are you sure you want to deaccession this dataset? It will no longer be viewable by the public.

Version Differences Details

Please select two versions to view the differences.

Version Differences Details
 
Version:
Last Updated:
Version:
Last Updated:
Select File(s)

Please select a file or files to be downloaded.

Select File(s)

Please select a file or files for access request.

Edit Tags

Select existing file tags or create new tags to describe your files. Each file can have more than one tag.

Request Access

  You need to Sign Up or Log In to request access to this file.

???file.mapData.unpublished.header???

???file.mapData.unpublished.message???

Dataset Terms

Please confirm and/or complete the information needed below in order to continue.

Terms of Access
File yang diunduh dari RIN ini mungkin tidak didistribusikan ulang dalam bentuk apapun (elektronik, elektro-magnetik atau cetak) tanpa izin dari distributor data sebelumnya. Dengan mendownload file, saya mengonfirmasi bahwa saya telah membaca dan memahami setiap istilah yang ditetapkan dalam persyaratan dan ketentuan penggunaan data dan materi lain yang ditemukan di bawah ini, dan saya setuju untuk terikat oleh semua persyaratan dan ketentuan tersebut. Jika saya tidak mengerti atau menyetujui semua persyaratan dan ketentuan, saya tidak boleh menggunakan atau mendownload data atau materi lainnya.

-----------

Aturan dan Perilaku
Sebagai syarat penggunaan, Anda berjanji untuk tidak menggunakan Layanan untuk tujuan apa pun yang dilarang oleh Persyaratan Penggunaan. Untuk tujuan Persyaratan Penggunaan, "Konten" mencakup, tanpa batasan, informasi, data, teks, perangkat lunak, skrip, grafik, dan fitur interaktif apa pun yang dihasilkan, disediakan, atau dibuat dapat diakses oleh RIN atau mitranya pada atau melalui Layanan . Sebagai contoh, dan bukan sebagai batasan, Anda tidak boleh (atau mengizinkan orang lain untuk) melakukan (a) mengambil tindakan atau (b) mengunggah, mendownload, mengirim, mengirimkan atau mendistribusikan atau memfasilitasi distribusi konten apapun dengan menggunakan komunikasi apapun. layanan atau layanan lain yang tersedia pada atau melalui Layanan, bahwa:
  • melanggar hak paten, merek dagang, rahasia dagang, hak cipta, hak publisitas atau hak lain dari orang atau entitas lain;
  • melanggar hukum, mengancam, kasar, melecehkan, memfitnah, menipu, melanggar privasi orang lain, menyiksa, cabul, menyinggung, atau profan;
  • merupakan iklan yang tidak sah atau tidak diminta, spam atau e-mail massal ("spamming");
  • berisi virus perangkat lunak atau kode komputer, file, atau program lain yang dirancang atau dimaksudkan untuk mengganggu, merusak, membatasi atau mengganggu fungsi perangkat lunak, perangkat keras, atau perangkat telekomunikasi yang sesuai atau merusak atau mendapatkan akses tidak sah ke sistem apapun, data atau informasi lain dari RIN atau pihak ketiga; atau Selain itu, Anda tidak boleh: (i) mengambil tindakan yang memaksakan atau memaksakan (sebagaimana ditentukan oleh RIN atas kebijakannya sendiri) beban besar yang tidak masuk akal atau tidak proporsional terhadap infrastruktur RIN (atau penyedia pihak ketiga); (ii) mengganggu atau mencoba mengganggu pelaksanaan Layanan atau kegiatan yang dilakukan oleh Dinas; atau (iii) mengabaikan semua tindakan yang mungkin digunakan RIN untuk mencegah atau membatasi akses ke Layanan (atau akun lain, sistem komputer atau jaringan yang terhubung ke Layanan).
Anda harus mematuhi semua hukum dan peraturan lokal, negara bagian, nasional dan internasional yang berlaku.
Preview Guestbook

Upon downloading files the guestbook asks for the following information.

Account Information

Package File Download

Use the Download URL in a Wget command or a download manager to download this package file. Download via web browser is not recommended. User Guide - Downloading a Dataverse Package via URL

-

https://data.brin.go.id/api/access/datafile/

Request Access

Please confirm and/or complete the information needed below in order to request access to files in this dataset.

File yang diunduh dari RIN ini mungkin tidak didistribusikan ulang dalam bentuk apapun (elektronik, elektro-magnetik atau cetak) tanpa izin dari distributor data sebelumnya. Dengan mendownload file, saya mengonfirmasi bahwa saya telah membaca dan memahami setiap istilah yang ditetapkan dalam persyaratan dan ketentuan penggunaan data dan materi lain yang ditemukan di bawah ini, dan saya setuju untuk terikat oleh semua persyaratan dan ketentuan tersebut. Jika saya tidak mengerti atau menyetujui semua persyaratan dan ketentuan, saya tidak boleh menggunakan atau mendownload data atau materi lainnya.

-----------

Aturan dan Perilaku
Sebagai syarat penggunaan, Anda berjanji untuk tidak menggunakan Layanan untuk tujuan apa pun yang dilarang oleh Persyaratan Penggunaan. Untuk tujuan Persyaratan Penggunaan, "Konten" mencakup, tanpa batasan, informasi, data, teks, perangkat lunak, skrip, grafik, dan fitur interaktif apa pun yang dihasilkan, disediakan, atau dibuat dapat diakses oleh RIN atau mitranya pada atau melalui Layanan . Sebagai contoh, dan bukan sebagai batasan, Anda tidak boleh (atau mengizinkan orang lain untuk) melakukan (a) mengambil tindakan atau (b) mengunggah, mendownload, mengirim, mengirimkan atau mendistribusikan atau memfasilitasi distribusi konten apapun dengan menggunakan komunikasi apapun. layanan atau layanan lain yang tersedia pada atau melalui Layanan, bahwa:
  • melanggar hak paten, merek dagang, rahasia dagang, hak cipta, hak publisitas atau hak lain dari orang atau entitas lain;
  • melanggar hukum, mengancam, kasar, melecehkan, memfitnah, menipu, melanggar privasi orang lain, menyiksa, cabul, menyinggung, atau profan;
  • merupakan iklan yang tidak sah atau tidak diminta, spam atau e-mail massal ("spamming");
  • berisi virus perangkat lunak atau kode komputer, file, atau program lain yang dirancang atau dimaksudkan untuk mengganggu, merusak, membatasi atau mengganggu fungsi perangkat lunak, perangkat keras, atau perangkat telekomunikasi yang sesuai atau merusak atau mendapatkan akses tidak sah ke sistem apapun, data atau informasi lain dari RIN atau pihak ketiga; atau Selain itu, Anda tidak boleh: (i) mengambil tindakan yang memaksakan atau memaksakan (sebagaimana ditentukan oleh RIN atas kebijakannya sendiri) beban besar yang tidak masuk akal atau tidak proporsional terhadap infrastruktur RIN (atau penyedia pihak ketiga); (ii) mengganggu atau mencoba mengganggu pelaksanaan Layanan atau kegiatan yang dilakukan oleh Dinas; atau (iii) mengabaikan semua tindakan yang mungkin digunakan RIN untuk mencegah atau membatasi akses ke Layanan (atau akun lain, sistem komputer atau jaringan yang terhubung ke Layanan).
Anda harus mematuhi semua hukum dan peraturan lokal, negara bagian, nasional dan internasional yang berlaku.
Compute Batch
Clear Batch
Dataset Dataset Persistent ID
Compute Batch
Submit for Review

You will not be able to make changes to this dataset while it is in review.

Publish Dataset

Are you sure you want to republish this dataset?

Select if this is a minor or major version update.

Publish Dataset

This dataset cannot be published until Prosiding Dataverse is published by its administrator.

Publish Dataset

This dataset cannot be published until Prosiding Dataverse and Karya Ilmiah Dataverse are published.

Return to Author

Return this dataset to contributor for modification.

Contact RIN Dataverse Support

RIN Dataverse Support

Please fill this out to prove you are not a robot.

+ =