Sintesis Material Nanokristalin Bpscco Melalui Metode Pencampuran Basah

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Siswayanti, Bintoro; Yudanto, Sigit Dwi; Imaduddin, Agung; Lusiana; Sebleku, Pius, 2018, "Sintesis Material Nanokristalin Bpscco Melalui Metode Pencampuran Basah", https://hdl.handle.net/20.500.12690/RIN/IBUWIG, RIN Dataverse, V1

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Description

Bismuth Strontium Calcium Copper Oxide (BSCCO) merupakan material superkonduktor. Pada penelitian ini dilakukan sintesis material superkonduktor BPSCCO menggunakan metode pencampuran basah untuk mendapatkan kristal berukuran nano. Percobaan sintesis material BPSCCO menggunakan bahan baku serbuk Bi2O3, Pb(NO3)2, SrCO3, CaO dan CuO. Bahan baku dicampur sesuai stoikiometri Bi2223 kemudian dilarutkan dalam HNO3 dan akuades. Larutan diaduk sambil dipanaskan dengan suhu 180 - 200°C selama 1 jam kemudian suhu dinaikkan menjadi 200 - 250°C sampai larutan menjadi kering. Padatan yang diperoleh ditambahkan aceton dan selanjutnya digerus dengan menggunakan high energy miller selama 30 menit. Campuran yang sudah digerus dikeringkan dan dikalsinasi dengan suhu 820°C selama 20 jam. Hasil kalsinasi dibentuk pelet dan disinter dengan suhu 880°C yang ditahan selama 80 jam. Hasil difraksi sinar-X menunjukkan bahwa fasa yang terbentuk berupa fasa Bi2212 sedangkan Bi2223 tidak ditemukan. Ukuran kristal yang terbentuk didekati dengan persamaan Debye Scherer bernilai 0.8143 nm.

Prosiding Seminar Material Metalurgi 2014

(2014)

Subject

Chemistry


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Citation Metadata

Dataset Persistent ID	hdl:20.500.12690/RIN/IBUWIG
Publication Date	2018-04-08
Title	Sintesis Material Nanokristalin Bpscco Melalui Metode Pencampuran Basah
Author	Siswayanti, Bintoro (Pusat Penelitian Metalurgi dan Material) Yudanto, Sigit Dwi (Pusat Penelitian Metalurgi dan Material) Imaduddin, Agung (Pusat Penelitian Metalurgi dan Material) Lusiana (Pusat Penelitian Metalurgi dan Material) Sebleku, Pius (Pusat Penelitian Metalurgi dan Material)
Contact	Use email button above to contact. Siswayanti, Bintoro (Pusat Penelitian Metalurgi dan Material)
Description	Bismuth Strontium Calcium Copper Oxide (BSCCO) merupakan material superkonduktor. Pada penelitian ini dilakukan sintesis material superkonduktor BPSCCO menggunakan metode pencampuran basah untuk mendapatkan kristal berukuran nano. Percobaan sintesis material BPSCCO menggunakan bahan baku serbuk Bi2O3, Pb(NO3)2, SrCO3, CaO dan CuO. Bahan baku dicampur sesuai stoikiometri Bi2223 kemudian dilarutkan dalam HNO3 dan akuades. Larutan diaduk sambil dipanaskan dengan suhu 180 - 200°C selama 1 jam kemudian suhu dinaikkan menjadi 200 - 250°C sampai larutan menjadi kering. Padatan yang diperoleh ditambahkan aceton dan selanjutnya digerus dengan menggunakan high energy miller selama 30 menit. Campuran yang sudah digerus dikeringkan dan dikalsinasi dengan suhu 820°C selama 20 jam. Hasil kalsinasi dibentuk pelet dan disinter dengan suhu 880°C yang ditahan selama 80 jam. Hasil difraksi sinar-X menunjukkan bahwa fasa yang terbentuk berupa fasa Bi2212 sedangkan Bi2223 tidak ditemukan. Ukuran kristal yang terbentuk didekati dengan persamaan Debye Scherer bernilai 0.8143 nm. Prosiding Seminar Material Metalurgi 2014 (2014)
Subject	Chemistry
Depositor	Medina, Dyta
Deposit Date	2018-04-08

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